C₃₀H₃₆N₆OSi

Base Information

Chemical Name:C₃₀H₃₆N₆OSi
CAS No.:1202036-41-6
Molecular Formula:C₃₀H₃₆N₆OSi
Molecular Weight:524.741
Hs Code.:

C<sub>30</sub>H<sub>36</sub>N<sub>6</sub>OSi

Synonyms:C₃₀H₃₆N₆OSi

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Chemical Property of C₃₀H₃₆N₆OSi

Chemical Property:

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Technology Process of C₃₀H₃₆N₆OSi

There total 6 articles about C₃₀H₃₆N₆OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6307-83-1
3-bromo-5-nitro-benzoic acid

: 1202036-41-6
C₃₀H₃₆N₆OSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: borane-THF / tetrahydrofuran / 0 - 20 °C

1.2: 0 °C

2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 - 20 °C

2.2: 16 h / 20 °C

3.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 0.17 h / 120 °C

4.1: hydrogen / Raney Ni / methanol / 5 h / Inert atmosphere of nitrogen

5.1: hydrogenchloride / 1,4-dioxane; isopropyl alcohol / 110 °C

6.1: copper(l) iodide; triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 0.33 h / 120 °C

With hydrogenchloride; copper(l) iodide; borane-THF; hydrogen; sodium carbonate; methanesulfonyl chloride; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 1202034-53-4
6-bromo-N-(3-((2,6-dimethylmorpholino)methyl)-5-(1-methyl-1H-pyrazol-4-yl)phenyl)quinazolin-2-amine

: 1066-54-2
trimethylsilylacetylene

: 1202036-41-6
C₃₀H₃₆N₆OSi

Guidance literature:: With copper(l) iodide; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In N,N-dimethyl-formamide; at 120 ℃; for 0.333333h;

Reference yield:

: 1202036-22-3
4-(3-bromo-5-nitrobenzyl)-2,6-dimethylmorpholine

: 1202036-41-6
C₃₀H₃₆N₆OSi

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 0.17 h / 120 °C

2: hydrogen / Raney Ni / methanol / 5 h / Inert atmosphere of nitrogen

3: hydrogenchloride / 1,4-dioxane; isopropyl alcohol / 110 °C

4: copper(l) iodide; triethylamine / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 0.33 h / 120 °C

With hydrogenchloride; copper(l) iodide; hydrogen; sodium carbonate; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; isopropyl alcohol;