methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

Base Information

Chemical Name:methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate
CAS No.:1259286-14-0
Molecular Formula:C₁₄H₂₁NO₄S
Molecular Weight:299.391
Hs Code.:

Synonyms:methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

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Chemical Property of methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

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Technology Process of methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

There total 3 articles about methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1259286-13-9
methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylthio)butanoate

: 1259286-14-0
methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

Guidance literature:: With sodium periodate; In methanol; water; at 20 ℃; for 3.5h; Cooling with ice;
DOI:10.1021/jo101790z

Reference yield:

: 2491-18-1
(S)-methyl 2-amino-4-(methylthio)butanoate hydrochloride

: 1259286-14-0
methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 19 h / 20 °C / Inert atmosphere

2: sodium periodate / methanol; water / 3.5 h / 20 °C / Cooling with ice

With sodium periodate; sodium tris(acetoxy)borohydride; triethylamine; In methanol; water; 1,2-dichloro-ethane;
DOI:10.1021/jo101790z

Reference yield:

: 63-68-3,26062-47-5,58576-49-1
L-methionine

: 1259286-14-0
methyl (2S)-2-[[(4-methoxyphenyl)methyl]amino]-4-(methylsulfinyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride / Reflux

2: sodium tris(acetoxy)borohydride; triethylamine / 1,2-dichloro-ethane / 19 h / 20 °C / Inert atmosphere

3: sodium periodate / methanol; water / 3.5 h / 20 °C / Cooling with ice

With sodium periodate; sodium tris(acetoxy)borohydride; triethylamine; acetyl chloride; In methanol; water; 1,2-dichloro-ethane;
DOI:10.1021/jo101790z