(1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

Base Information

Chemical Name:(1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione
CAS No.:1356917-45-7
Molecular Formula:C₂₄H₂₂O₆
Molecular Weight:406.435
Hs Code.:

Synonyms:(1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

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Chemical Property of (1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

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Technology Process of (1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

There total 2 articles about (1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 38352-74-8
3-acetylhex-5-yn-2-one

: 121-33-5,8014-42-4
vanillin

: 1356917-45-7
(1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

Guidance literature:: 3-acetylhex-5-yn-2-one; With boron trioxide; In ethyl acetate; at 40 ℃; for 0.5h; Inert atmosphere;

vanillin; With boric acid tributyl ester; In ethyl acetate; at 40 ℃; for 0.5h;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 106-96-7
propargyl bromide

: 123-54-6,81235-32-7
acetylacetone

: 1356917-45-7
(1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

: 1240264-80-5
(1E,4Z,6E)-5-hydroxy-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,4,6-trien-3-one

Guidance literature:: propargyl bromide; acetylacetone; With potassium carbonate; In acetone; toluene; at 80 ℃; for 6h;

With boron trioxide; In N,N-dimethyl-formamide; at 80 ℃; for 0.5h;

vanillin; Further stages;
DOI:10.3390/molecules25133066

Reference yield:

: 1356917-45-7
(1E,6E)-1,7-bis(4-hydroxy-3-methoxyphenyl)-4-(prop-2-yn-1-yl)hepta-1,6-diene-3,5-dione

: C₆₀H₁₀₇N₁₁O₅

: C₈₄H₁₂₉N₁₁O₁₁

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; Inert atmosphere;
DOI:10.1016/j.bmcl.2018.02.028