diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate

Base Information

Chemical Name:diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate
CAS No.:1310479-96-9
Molecular Formula:C₁₆H₂₇F₂O₃PSi
Molecular Weight:364.445
Hs Code.:

Synonyms:diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate

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Technology Process of diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate

There total 1 articles about diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 75-77-4
chloro-trimethyl-silane

: 1310480-08-0
diethyl 2-(difluoromethyl)-4,5-dimethylphenylphosphonate

: 1310479-96-9
diethyl 2-[difluoro(trimethylsilyl)methyl]-4,5-dimethylphenylphosphonate

Guidance literature:: diethyl 2-(difluoromethyl)-4,5-dimethylphenylphosphonate; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -80 ℃; for 0.5h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; pentane; at 0 - 5 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2011.03.076