benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

Base Information

Chemical Name:benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate
CAS No.:955936-62-6
Molecular Formula:C₂₃H₂₈N₂O₄S
Molecular Weight:428.552
Hs Code.:

Synonyms:benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

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Chemical Property of benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

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Technology Process of benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

There total 1 articles about benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-84-1
O-benzyl carbamate

: 220384-55-4
1-(p-toluenesulfonyl)-piperidin-3-one

: 762-72-1
allyl-trimethyl-silane

: 955936-62-6
benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 23 ℃; for 9h;
DOI:10.1016/j.tet.2007.07.083

Reference yield: 50.0%

: 955936-62-6
benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

: 4224-69-5
methyl 2-(bromomethyl)propenoate

: 955936-63-7
methyl 2-[([(benzyloxy)carbonyl]{1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}amino)methyl]prop-2-enoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 23 ℃;
DOI:10.1016/j.tet.2007.07.083

Reference yield:

: 955936-62-6
benzyl {1-[(4-methylphenyl)sulfonyl]-3-prop-2-en-1-ylpiperidin-3-yl}carbamate

: 955936-64-8
1-benzyl 3-methyl 8-[(4-methylphenyl)sulfonyl]-1,8-diazaspiro[5.5]undec-3-ene-1,3-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / NaH / tetrahydrofuran; dimethylformamide / 0 - 23 °C

2: 65 percent / second generation Grubbs catalyst / CH₂Cl₂ / 4 h / Heating

With sodium hydride; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.07.083