1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide

Base Information

• Chemical Name: 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide
• CAS No.: 432555-99-2
• Molecular Formula: C₃₀H₃₆N₂O₁₀
• Molecular Weight: 584.623

Synonyms:1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide

Chemical Property of 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide

There total 2 articles about 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

H-Phe-OEt (3081-24-1) + 2,3-diacetoxy-(2S,3S)-butanedioic acid dichloride → 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide (432555-99-2)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1016/S0014-827X(02)00016-2

Reference yield:

2,3-diacetoxy-(2S,3S)-butanedioic acid (66749-60-8) → 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide (432555-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (COCl)2 / dimethylformamide; CH₂Cl₂ / 2 h / 20 °C

2: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

With oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0014-827X(02)00016-2

Reference yield: 80.0%

1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide (432555-99-2) → 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-dihydroxy-(2S,3S)-butanediamide

Guidance literature:

With sulfuric acid; In ethanol; for 4h; Heating;

DOI:10.1016/S0014-827X(02)00016-2

upstream raw materials:

H-Phe-OEt

2,3-diacetoxy-(2S,3S)-butanedioic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 432555-99-2 1N,4N-di[1-carboethoxy-2-phenyl-(1S)-ethyl]-2,3-diacetoxy-(2S,3S)-butanediamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send