C₁₅H₉N₃

Base Information

Chemical Name:C₁₅H₉N₃
CAS No.:1401421-09-7
Molecular Formula:C₁₅H₉N₃
Molecular Weight:231.257
Hs Code.:

C<sub>15</sub>H<sub>9</sub>N<sub>3</sub>

Synonyms:C₁₅H₉N₃

Suppliers and Price of C₁₅H₉N₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₉N₃

Chemical Property:

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Technology Process of C₁₅H₉N₃

There total 3 articles about C₁₅H₉N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1401421-37-1
C₁₆H₁₅N₃

: 1401421-09-7
C₁₅H₉N₃

Guidance literature:: With pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; copper(II) sulfate; In N,N-dimethyl-formamide; at 150 ℃; for 20h; under 760.051 Torr;
DOI:10.1002/anie.201204339

Reference yield:

: 98-86-2
acetophenone

: 1401421-09-7
C₁₅H₉N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / ethanol / Reflux

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

2.2: 5 h / 0 °C / Reflux

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 20 h / 120 - 150 °C / Inert atmosphere

4.1: pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; copper(II) sulfate / N,N-dimethyl-formamide / 20 h / 150 °C / 760.05 Torr

With pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; sodium hydride; copper(II) sulfate; acetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201204339

Reference yield:

: 589-21-9
(4-bromophenyl)hydrazine

: 1401421-09-7
C₁₅H₉N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / ethanol / Reflux

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

2.2: 5 h / 0 °C / Reflux

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 20 h / 120 - 150 °C / Inert atmosphere

4.1: pyridine; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; copper(II) sulfate / N,N-dimethyl-formamide / 20 h / 150 °C / 760.05 Torr

With pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; trifluorormethanesulfonic acid; oxygen; sodium hydride; copper(II) sulfate; acetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201204339