3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

Base Information

Chemical Name:3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole
CAS No.:1332498-26-6
Molecular Formula:C₂₉H₄₂N₂O₃Si₂
Molecular Weight:522.835
Hs Code.:

Synonyms:3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

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Chemical Property of 3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

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Technology Process of 3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

There total 4 articles about 3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19227-11-3
N'-hydroxy-2-phenylethanimidamide

: 141818-62-4
C₂₁H₃₅ClO₃Si₂

: 1332498-26-6
3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

Guidance literature:: With pyridine; In xylene; at 130 - 140 ℃;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1332498-26-6
3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 72 h / 20 °C

1.2: 0.75 h / 20 °C / pH ~ 8

1.3: 0 °C / pH 6

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C

3.1: pyridine / xylene / 130 - 140 °C

With pyridine; 1H-imidazole; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide; xylene;

Reference yield:

: 331-39-5,501-16-6
caffeic acid

: 1332498-26-6
3-benzyl-5-{2-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)phenyl]-vinyl}-[1,2,4]oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 72 h / 20 °C

1.2: 0.75 h / 20 °C / pH ~ 8

1.3: 0 °C / pH 6

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C

3.1: pyridine / xylene / 130 - 140 °C

With pyridine; 1H-imidazole; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide; xylene;