5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

Base Information

Chemical Name:5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid
CAS No.:1189797-80-5
Molecular Formula:C₁₁H₁₁BrN₂O₄S
Molecular Weight:347.189
Hs Code.:

Synonyms:5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

Suppliers and Price of 5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

There total 1 articles about 5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 16182-04-0
Ethoxycarbonyl isothiocyanate

: 5794-88-7
5-Bromo-2-aminobenzoic acid

: 1189797-80-5
5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

Guidance literature:: In acetonitrile; at 80 ℃; for 5h;
DOI:10.1016/j.bmc.2010.11.050

Reference yield:

: 1189797-80-5
5-bromo-2-({[(ethoxycarbonyl)amino]carbonothioyl}-amino)-benzoic acid

: 49681-96-1
6-bromo-2,3-dihydro-2-thioxo-quinazolin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 4 h / 60 °C

2.1: sodium methylate / tetrahydrofuran; methanol / 1.5 h / Reflux

2.2: 20 °C

With sodium methylate; acetic anhydride; In tetrahydrofuran; methanol;