bis(trimethylsilyl)methan

Base Information

• Chemical Name: bis(trimethylsilyl)methan
• CAS No.: 78907-64-9
• Molecular Formula: C₁₅H₃₀SSi₃
• Molecular Weight: 326.726
• Mol file: 78907-64-9.mol

Synonyms:bis(trimethylsilyl)methan

Chemical Property of bis(trimethylsilyl)methan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(trimethylsilyl)methan

There total 7 articles about bis(trimethylsilyl)methan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan (80431-36-3) + thiophenol (108-98-5) → Benzophenone imine (1013-88-3) + phenylthiotrimethylsilane (4551-15-9) + bis(trimethylsilyl)methan (78907-64-9)

Guidance literature:

In diethyl ether; at 100 ℃; for 5h;

Reference yield:

C15H29LiSSi3 (78907-52-5) → bis(trimethylsilyl)methan (78907-64-9)

Guidance literature:

With t-butyl bromide; In diethyl ether; benzene; at -78 ℃;

Reference yield:

dibromobis(trimethylsilyl)methane (29955-10-0) → bis(trimethylsilyl)methan (78907-64-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 95 percent / BuLi / tetrahydrofuran; hexane; diethyl ether / -115 deg C to r.t.

2: 96 percent / Br₂ / 2 h / 60 °C

3: 51 percent / tetrahydrofuran

4: PhLi / diethyl ether; benzene / -78 °C / BuLi

5: t-BuBr / diethyl ether; benzene / -78 °C

With n-butyllithium; t-butyl bromide; bromine; phenyllithium; In tetrahydrofuran; diethyl ether; hexane; benzene;

upstream raw materials:

2,2-Dimethyl-4,4-diphenyl-1,3,3-tris(trimethylsilyl)-1-aza-2-silacyclobutan

thiophenol

C₁₅H₂₉LiSSi₃

dibromobis(trimethylsilyl)methane