methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

Base Information

Chemical Name:methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate
CAS No.:1609575-61-2
Molecular Formula:C₁₆H₁₇F₆NO₃
Molecular Weight:385.306
Hs Code.:

Synonyms:methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

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Chemical Property of methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

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Technology Process of methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

There total 1 articles about methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 30914-89-7
2-(3-(trifluoromethyl)phenyl)morpholine

: 382-90-1
methyl α-trifluoromethylacrylate

: 1609575-61-2
methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

Guidance literature:: at 20 ℃; for 0.833333h;

Reference yield: 98.0%

: 1609575-61-2
methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

: 3,3,3-trifluoro-2-[2-(3-trifluoromethyl-phenyl)-morpholin-4-ylmethyl]-propan-1-ol

Guidance literature:: methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate; With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 1h;

With sodium hydroxide; In tetrahydrofuran; diethyl ether; water; at 0 ℃; for 0.333333h;

Reference yield:

: 1609575-61-2
methyl 3,3,3-trifluoro-2-((2-(3-(trifluoromethyl)phenyl)morpholino)-methyl)propanoate

: 1609575-64-5
4,4,4-trifluoro-3-[2-(3-trifluoromethylphenyl)-morpholin-4-ylmethyl]-butyronitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether; tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 0.33 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

3.1: N,N-dimethyl-formamide / 2 h / 60 °C

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;