(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

Base Information

Chemical Name:(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide
CAS No.:1377823-84-1
Molecular Formula:C₂₈H₃₇F₃N₂O₄S
Molecular Weight:554.674
Hs Code.:

Synonyms:(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

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Chemical Property of (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

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Technology Process of (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

There total 8 articles about (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1352790-95-4
(S)-2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)-1,3-oxazolidine-4-carbaldehyde

: 102512-07-2
N-(4-(trifluoromethyl)phenyl)hydroxylamine

: 1377823-84-1
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 - 25 ℃;
DOI:10.1021/ol300982f

Reference yield:

: 1377823-82-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

: 1377823-84-1
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2: hydrogenchloride; water / tetrahydrofuran / 4 h / -78 - 25 °C / Inert atmosphere

3: magnesium sulfate / dichloromethane / 20 - 25 °C

With hydrogenchloride; water; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300982f

Reference yield:

: C₄₀H₅₂N₂O₆S

: 1377823-84-1
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / tetrahydrofuran / 4 h / -78 - 25 °C / Inert atmosphere

2: magnesium sulfate / dichloromethane / 20 - 25 °C

With hydrogenchloride; water; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300982f