(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

Base Information

Chemical Name:(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide
CAS No.:1377823-82-9
Molecular Formula:C₂₇H₃₇FN₂O₄S
Molecular Weight:504.666
Hs Code.:

Synonyms:(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

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Chemical Property of (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

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Technology Process of (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

There total 10 articles about (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352790-95-4
(S)-2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)-1,3-oxazolidine-4-carbaldehyde

: 406-00-8
4-fluoro-N-hydroxyaniline

: 1377823-82-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 - 25 ℃;
DOI:10.1021/ol300982f

Reference yield:

: 1377823-84-1
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

: 1377823-82-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2: hydrogenchloride; water / tetrahydrofuran / 4 h / -78 - 25 °C / Inert atmosphere

3: magnesium sulfate / dichloromethane / 20 - 25 °C

With hydrogenchloride; water; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300982f

Reference yield:

: C₄₀H₅₂N₂O₆S

: 1377823-82-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / tetrahydrofuran / 4 h / -78 - 25 °C / Inert atmosphere

2: magnesium sulfate / dichloromethane / 20 - 25 °C

With hydrogenchloride; water; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300982f