(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

Base Information

Chemical Name:(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide
CAS No.:1377823-90-9
Molecular Formula:C₂₈H₄₀N₂O₄S
Molecular Weight:500.703
Hs Code.:

Synonyms:(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

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Chemical Property of (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

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Technology Process of (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

There total 16 articles about (R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1352790-95-4
(S)-2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)-1,3-oxazolidine-4-carbaldehyde

: 611-22-3
N-(o-tolyl)hydroxylamine

: 1377823-90-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 0.0833333h;
DOI:10.1039/c4ob02526a

Reference yield:

: 1377823-84-1
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-(trifluoromethyl)aniline oxide

: 1377823-90-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2: hydrogenchloride; water / tetrahydrofuran / 4 h / -78 - 25 °C / Inert atmosphere

3: magnesium sulfate / dichloromethane / 20 - 25 °C

With hydrogenchloride; water; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300982f

Reference yield:

: 1377823-82-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-4-fluoroaniline oxide

: 1377823-90-9
(R,Z)-N-((2,2-dimethyl-3-((2,4,6-triisopropylphenyl)sulfonyl)oxazolidin-4-yl)methylene)-2-methylaniline oxide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2: hydrogenchloride; water / tetrahydrofuran / 4 h / -78 - 25 °C / Inert atmosphere

3: magnesium sulfate / dichloromethane / 20 - 25 °C

With hydrogenchloride; water; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol300982f