3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

Base Information

Chemical Name:3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide
CAS No.:1200439-41-3
Molecular Formula:C₂₃H₂₅N₇O₂
Molecular Weight:431.497
Hs Code.:

Synonyms:3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

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Chemical Property of 3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

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Technology Process of 3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

There total 5 articles about 3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200440-12-5
3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-propionic acid

: 3528-45-8
1-(4-methoxybenzyl)-1H-pyrazol-5-amine

: 1200439-41-3
3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1200439-41-3
3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 2 h / 70 °C

2: sodium t-butanolate / isopropyl alcohol / 4 h / 110 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium t-butanolate; In ethanol; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 359447-00-0
N-(2,3-dimethyl-phenyl)-succinamic acid ethyl ester

: 1200439-41-3
3-[1-(2,3-dimethyl-phenyl)-1H-tetrazol-5-yl]-N-[2-(4-methoxy-benzyl)-2H-pyrazol-3-yl]-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilylazide; triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C

2: sodium hydroxide; water / tetrahydrofuran; methanol / 18 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 18 h / 20 °C

With dmap; trimethylsilylazide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; diisopropyl azodicarboxylate; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;