2-(cyclohexylimino)-3-nitrosothiazolidine

Base Information

• Chemical Name: 2-(cyclohexylimino)-3-nitrosothiazolidine
• CAS No.: 87191-81-9
• Molecular Formula: C₉H₁₅N₃OS
• Molecular Weight: 213.304
• Mol file: 87191-81-9.mol

Synonyms:2-(cyclohexylimino)-3-nitrosothiazolidine

Chemical Property of 2-(cyclohexylimino)-3-nitrosothiazolidine

Chemical Property:

Purity/Quality:

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Technology Process of 2-(cyclohexylimino)-3-nitrosothiazolidine

There total 13 articles about 2-(cyclohexylimino)-3-nitrosothiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-(cyclohexylimino)thiazolidine (56242-66-1) → 2-(cyclohexylimino)-3-nitrosothiazolidine (87191-81-9)

Guidance literature:

With n-Butyl nitrite; sodium methylate; In diethyl ether;

DOI:10.1021/jo00170a006

Reference yield: 73.0%

N-cyclohexyl-4,5-dihydro-1,3-thiazol-2-amine (56242-66-1) → 2-(cyclohexylimino)-3-nitrosothiazolidine (87191-81-9)

Guidance literature:

With n-Butyl nitrite; sodium methylate; In diethyl ether; at 0 - 5 ℃;

Reference yield: 20.0%

N3-cyclohexyl-N1-(2-fluoroethyl)-N1-nitrosothiourea (79645-05-9) → N-cyclohexyl-4,5-dihydro-1,3-thiazol-2-amine (56242-66-1) + 2-fluoroethanol (371-62-0) + 2-(cyclohexylimino)-3-nitrosothiazolidine (87191-81-9) + isothiocyanatocyclohexane (1122-82-3)

Guidance literature:

With potassium phosphate buffer; at 37 ℃; for 12h; Product distribution; Mechanism; decomposition by var. pH;

DOI:10.1021/jo00170a006

upstream raw materials:

N-cyclohexyl-4,5-dihydro-1,3-thiazol-2-amine

N₃-cyclohexyl-N₁-(2-fluoroethyl)-N₁-nitrosothiourea

2-(cyclohexylimino)thiazolidine

cyclohexylamine