(Fe(II))2(gable porphyrin)

Base Information

Chemical Name:(Fe(II))2(gable porphyrin)
CAS No.:96481-89-9
Molecular Formula:C₈₂H₅₀Fe₂N₈
Molecular Weight:1259.05
Hs Code.:

Synonyms:(Fe(II))2(gable porphyrin)

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Chemical Property of (Fe(II))2(gable porphyrin)

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Technology Process of (Fe(II))2(gable porphyrin)

There total 1 articles about (Fe(II))2(gable porphyrin) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96502-29-3
(C₆H₄(C₂₀H₈N₄(C₆H₅)3Fe)2)Cl₂

: 96481-89-9
(Fe(II))2(gable porphyrin)

Guidance literature:: With sodium dithionite; In water; benzene; a mixt. of Fe(III)-complex in benzene and aq. buffer (0.1 M phosphate, pH 6.86) was deoxygenated by 3 freeze-pump-thaw cycles in a dry-box withAr, solid Na2S2O4 added, mixt. was stirred vigorously for 30 min; dried over anhyd. Na2SO4 in a dry-box, applied to an alumina column (pretreated with Na2S2O4 in water under Ar followed by washing with H2O anddrying in vacuo for 12 h), eluted with O2-free MeOH (1%) in benzene; purity was checked by UV;
DOI:10.1021/ja00300a019