[Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

Base Information

Chemical Name:[Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]
CAS No.:86217-37-0
Molecular Formula:C₃₂H₂₉Cl₂P₃Pt
Molecular Weight:772.49
Hs Code.:

[Pt(((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)2PC<sub>6</sub>H<sub>5</sub>)Cl<sub>2</sub>]

Synonyms:[Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

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Chemical Property of [Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

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Technology Process of [Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

There total 1 articles about [Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 2071-24-1
bis(diphenylphosphinomethyl)phenylphosphine

: 86217-37-0
[Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

Guidance literature:: In dichloromethane; a soln. of ligand was added to complex, mixt. was stirred at room temp.for 1 h; soln. was concd., ethyl ether was added, ppt. was filtered, washed withethyl ether; elem.anal.;

Reference yield: 95.0%

: 86217-37-0
[Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

: 93842-01-4
[Pt(((C₆H₅)2PCH₂)2PC₆H₅)(CN)2]*CH₂Cl₂

Guidance literature:: With sodium cyanide; In ethanol; dichloromethane; a soln. of complex in 1:1 mixt. of CH2Cl2 and EtOH was added to ethanolsoln. of NaCN, mixt. was heated under reflux for 8 h; mixt. was cooled, soln. was concd., mixt. was cooled in an ice bath, ppt. was filtered, washed with ethyl ether; elem.anal.;

Reference yield: 93.0%

: 86217-37-0
[Pt(((C₆H₅)2PCH₂)2PC₆H₅)Cl₂]

: 917-54-4
methyllithium

: 93862-09-0
[Pt(((C₆H₅)2PCH₂)2PC₆H₅)(CH₃)2]

Guidance literature:: With ammonium chloride; In diethyl ether; water; excess MeLi was added to a suspn. of complex in ethyl ether, which had been cooled to 0°C, mixt. was stirred for 1 h at 0°C, the soln. of NH4Cl in water was added; ether was sepd., mixt. was washed with CH2Cl2, soln. was evapd., ppt. was recrystd. from CH2Cl2 and MeOH, washed with MeOH; elem.anal.;