C₄₅H₆₆O₈Si₂

Base Information

Chemical Name:C₄₅H₆₆O₈Si₂
CAS No.:1609691-99-7
Molecular Formula:C₄₅H₆₆O₈Si₂
Molecular Weight:791.185
Hs Code.:

C<sub>45</sub>H<sub>66</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₄₅H₆₆O₈Si₂

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Chemical Property of C₄₅H₆₆O₈Si₂

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Technology Process of C₄₅H₆₆O₈Si₂

There total 8 articles about C₄₅H₆₆O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1609691-93-1
allyl 2-[2-{3,4-bis(triisopropylsilyloxy)benzyloxy}-3-(methoxymethoxy)phenyl]acetate

: 98-88-4
benzoyl chloride

: 1609691-99-7
C₄₅H₆₆O₈Si₂

Guidance literature:: allyl 2-[2-{3,4-bis(triisopropylsilyloxy)benzyloxy}-3-(methoxymethoxy)phenyl]acetate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1055/s-0033-1340291

Reference yield:

: 1126-20-1
2-allyloxyphenol

: 1609691-99-7
C₄₅H₆₆O₈Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 6 h / 50 °C / Inert atmosphere

2.1: 18 h / 180 °C / Microwave irradiation; Inert atmosphere

3.1: diethylazodicarboxylate; triphenylphosphine / toluene; tetrahydrofuran; diethyl ether / 6 h / 0 - 20 °C / Inert atmosphere

4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; diethyl ether; tert-butyl alcohol / 3 h / 0 - 20 °C

5.1: sodium periodate / water; diethyl ether / 6 h / 0 - 20 °C

6.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; diethyl ether; tert-butyl alcohol / 1.5 h

7.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 2 °C / Inert atmosphere

8.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

8.2: 1 h / -78 °C / Inert atmosphere

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; caesium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 2.1: |Claisen Rearrangement / 3.1: |Mitsunobu Displacement;
DOI:10.1055/s-0033-1340291

Reference yield:

: C₃₅H₅₈O₆Si₂

: 1609691-99-7
C₄₅H₆₆O₈Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; diethyl ether; tert-butyl alcohol / 1.5 h

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 2 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; caesium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1055/s-0033-1340291