2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

Base Information

Chemical Name:2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol
CAS No.:215780-27-1
Molecular Formula:C₂₇H₃₈OSi
Molecular Weight:406.684
Hs Code.:

Synonyms:2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

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Chemical Property of 2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

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Technology Process of 2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

There total 5 articles about 2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-16-1
methylmagnesium bromide

: 215780-18-0
5-Methyl-2-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hex-4-enoic acid ethyl ester

: 215780-27-1
2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

Guidance literature:: In tetrahydrofuran; diethyl ether; for 24h; Ambient temperature;

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 215780-27-1
2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / Cl₃SiH, Ph₃P / PdCl₂(PhCN)2 / 7 h / 70 °C

2: 70 percent / diethyl ether; cyclohexane / 1.) -78 deg C, 2 h, 2.) r.t., overnight

4: 80 percent / diethyl ether; tetrahydrofuran / 24 h / Ambient temperature

With trichlorosilane; triphenylphosphine; bis(benzonitrile)palladium(II) dichloride; In tetrahydrofuran; diethyl ether; cyclohexane;

Reference yield:

: 215033-01-5
chloro[(2Z)-2-methylbut-2-en-1-yl]diphenylsilane

: 215780-27-1
2,6-Dimethyl-3-{[((Z)-2-methyl-but-2-enyl)-diphenyl-silanyl]-methyl}-hept-5-en-2-ol

Guidance literature:: Multi-step reaction with 2 steps

2: 80 percent / diethyl ether; tetrahydrofuran / 24 h / Ambient temperature

In tetrahydrofuran; diethyl ether;