3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol

Base Information

Chemical Name:3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol
CAS No.:69343-73-3
Molecular Formula:C10H20 O2
Molecular Weight:172.268
Hs Code.:
European Community (EC) Number:273-972-9
UNII:454BR6L3BK
DSSTox Substance ID:DTXSID10989054
Nikkaji Number:J317.975C
Mol file:69343-73-3.mol

Synonyms:69343-73-3;3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol;EINECS 273-972-9;454BR6L3BK;DTXSID10989054;3-Methyl-2-(3-methyl-2-butenyl)-1,3-butanediol;3-Methyl-2-(3-methylbut-2-enyl)-butane-1,3-diol;3-Methyl-2-(3-methyl-2-buten-1-yl)-1,3-butanediol;1,3-Butanediol, 3-methyl-2-(3-methyl-2-buten-1-yl)-;3-METHYL-2-(3-METHYLBUT-2-EN-1-YL)BUTANE-1,3-DIOL

Suppliers and Price of 3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol

Chemical Property:

Vapor Pressure:0.000465mmHg at 25°C
Boiling Point:280.1°C at 760 mmHg
Flash Point:127°C
PSA：40.46000
Density:0.944g/cm³
LogP:1.72210
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:172.146329876
Heavy Atom Count:12
Complexity:155

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCC(CO)C(C)(C)O)C

Technology Process of 3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol

There total 10 articles about 3-Methyl-2-(3-methylbut-2-enyl)butane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 215780-28-2
1,1-Diphenyl-1-sila-2-oxa-3,3-dimethyl-4-(3-methylbut-2-enyl)cyclopentane

: 69343-73-3
3-methyl-2-(3-methyl-but-2-enyl)-butane-1,3-diol

Guidance literature:: With potassium fluoride; water; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; for 0.333333h; Ambient temperature;

Reference yield:

: 870-63-3
prenyl bromide

: 69343-73-3
3-methyl-2-(3-methyl-but-2-enyl)-butane-1,3-diol

Guidance literature:: Multi-step reaction with 5 steps

3: 80 percent / diethyl ether; tetrahydrofuran / 24 h / Ambient temperature

4: 80 percent / HCl, MeOH / CH₂Cl₂ / 0.02 h / Ambient temperature

5: 70 percent / H₂O₂, H₂O, KF, KHCO₃ / tetrahydrofuran; methanol / 0.33 h / Ambient temperature

With hydrogenchloride; methanol; potassium fluoride; water; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;

Reference yield:

: 54109-51-2
ethyl 5-methyl-2-methylenehex-4-enoate

: 69343-73-3
3-methyl-2-(3-methyl-but-2-enyl)-butane-1,3-diol

Guidance literature:: Multi-step reaction with 4 steps

2: 80 percent / diethyl ether; tetrahydrofuran / 24 h / Ambient temperature

3: 80 percent / HCl, MeOH / CH₂Cl₂ / 0.02 h / Ambient temperature

4: 70 percent / H₂O₂, H₂O, KF, KHCO₃ / tetrahydrofuran; methanol / 0.33 h / Ambient temperature

With hydrogenchloride; methanol; potassium fluoride; water; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;