N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

Base Information

Chemical Name:N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide
CAS No.:1207979-97-2
Molecular Formula:C₂₆H₁₆BrF₁₁N₂O₂
Molecular Weight:677.312
Hs Code.:

Synonyms:N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

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Chemical Property of N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

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Technology Process of N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

There total 10 articles about N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207727-04-5
3-[benzoyl(methyl)amino]-N-[2-bromo-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide

: 74-88-4
methyl iodide

: 1207979-97-2
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

Guidance literature:: 3-[benzoyl(methyl)amino]-N-[2-bromo-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.666667h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 6h;

Reference yield:

: 1207314-87-1
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

: 1207979-97-2
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium fluoride / N,N-dimethyl-formamide / 10 h / 130 °C / Inert atmosphere

2.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 4 h / 60 °C

2.2: pH 10

3.1: sulfuric acid / water / 40 °C

3.2: pH 10

4.1: pyridine / tetrahydrofuran / 5 h / 60 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / 20 °C

5.2: 6 h / 20 °C

With pyridine; hydrogenchloride; potassium fluoride; sulfuric acid; sodium hydride; tin(ll) chloride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1207314-88-2
N-[2-bromo-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-6-(trifluoromethyl)phenyl]-3-nitro-2-fluorobenzamide

: 1207979-97-2
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-fluoro-N-methyl-3-(N-methylbenzamide)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 4 h / 60 °C

1.2: pH 10

2.1: sulfuric acid / water / 40 °C

2.2: pH 10

3.1: pyridine / tetrahydrofuran / 5 h / 60 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / 20 °C

4.2: 6 h / 20 °C

With pyridine; hydrogenchloride; sulfuric acid; sodium hydride; tin(ll) chloride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;