N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

Base Information

Chemical Name:N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide
CAS No.:1207314-87-1
Molecular Formula:C₁₇H₆BrClF₁₀N₂O₃
Molecular Weight:591.587
Hs Code.:

Synonyms:N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

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Chemical Property of N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

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Technology Process of N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

There total 4 articles about N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1207314-86-0
2-bromo-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-6-(trifluoromethyl)aniline

: 34128-16-0
2-chloro-3-nitro-benzoyl chloride

: 1207314-87-1
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

Guidance literature:: 2-bromo-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-6-(trifluoromethyl)aniline; 2-chloro-3-nitro-benzoyl chloride; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -70 - 20 ℃; for 1h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield:

: 88-17-5
2-(trifluoromethyl)benzenamine

: 1207314-87-1
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium dithionite / ethyl acetate; water / 6 h / 20 °C

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 60 °C

3: lithium diisopropyl amide / hexane; tetrahydrofuran / 1 h / -70 - 20 °C

With N-Bromosuccinimide; sodium dithionite; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; lithium diisopropyl amide; In tetrahydrofuran; hexane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1207314-85-9
4-(perfluoropropane-2-yl)-2-(trifluoromethyl)aniline

: 1207314-87-1
N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-2-chloro-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 60 °C

2: lithium diisopropyl amide / hexane; tetrahydrofuran / 1 h / -70 - 20 °C

With N-Bromosuccinimide; lithium diisopropyl amide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;