2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide

Base Information

Chemical Name:2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide
CAS No.:1333327-13-1
Molecular Formula:C₁₆H₁₇BrN₂O₆
Molecular Weight:413.225
Hs Code.:

Synonyms:2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide

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Chemical Property of 2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide

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Technology Process of 2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide

There total 2 articles about 2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1333327-12-0
2-bromo-N-(1-hydroxymethyl-2-oxo-2-methoxyethyl)-N'-(2-oxo-2-ethoxyethyl)isophthalamide

: 1333327-13-1
2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide

Guidance literature:: 2-bromo-N-(1-hydroxymethyl-2-oxo-2-methoxyethyl)-N'-(2-oxo-2-ethoxyethyl)isophthalamide; With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; for 1h;

With potassium carbonate; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1039/c1dt10369e

Reference yield:

: 151603-30-4
2-bromobenzene-1,3-dicarboxylic acid dichloride

: 1333327-13-1
2-bromo-3-(4-methoxycarbonyloxazolin-2-yl)-N-(2-oxo-2-ethoxyethyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 12 h / -15 - 20 °C

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C

2.2: 1 h / -78 - 20 °C

With diethylamino-sulfur trifluoride; triethylamine; In dichloromethane;
DOI:10.1039/c1dt10369e