7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

Base Information

Chemical Name:7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin
CAS No.:474654-85-8
Molecular Formula:C₂₉H₄₄N₄O
Molecular Weight:464.695
Hs Code.:

Synonyms:7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

Chemical Property:

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Technology Process of 7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

There total 6 articles about 7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 474655-13-5
4-{(7-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-[4-(4-phenyl-piperazin-1-yl)-butyl]-amino}-butyronitrile

: 474654-85-8
7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1016/S0960-894X(01)00820-4

Reference yield:

: 92-54-6
4-phenyl-1-piperazine

: 474654-85-8
7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / dimethylformamide

2: hydrazine / ethanol

3: NaBH(OAc)3; AcOH / 1,2-dichloro-ethane

4: K₂CO₃ / dimethylformamide

5: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; hydrazine; In tetrahydrofuran; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(01)00820-4

Reference yield:

: 40255-41-2
4-(4-phenylpiperazin-1-yl)butan-1-amine

: 474654-85-8
7-Methoxyl-2-[N-(4-aminobutyl)-(N-(4-phenylpiperazin-1-yl)-butyl)amino]-tetralin

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH(OAc)3; AcOH / 1,2-dichloro-ethane

2: K₂CO₃ / dimethylformamide

3: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(01)00820-4