[Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl₂]

Base Information

• Chemical Name: [Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl₂]
• CAS No.: 1446446-15-6
• Molecular Formula: C₂₅H₁₄Cl₂CuN₄O
• Molecular Weight: 520.864

Synonyms:[Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl₂]

Chemical Property of [Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl₂]

Chemical Property:

Purity/Quality:

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Technology Process of [Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl₂]

There total 2 articles about [Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

copper(II) chloride monohydrate + (9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone (1220350-86-6) → [Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl2] (1446446-15-6)

Guidance literature:

With triethylamine; In ethanol; water; at 20 ℃; for 5h; Inert atmosphere; Reflux;

DOI:10.1016/j.saa.2013.04.124

Reference yield:

1,10-phenanthroline-5,6-dione (27318-90-7) + 4-benzoylbenzene-1,2-diamine (39070-63-8) → [Cu((9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone)Cl2] (1446446-15-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / Reflux

2: triethylamine / ethanol; water / 5 h / 20 °C / Inert atmosphere; Reflux

With triethylamine; In ethanol; water;

DOI:10.1016/j.saa.2013.04.124

upstream raw materials:

(9a,13a-dihydro-4,5,9,14-tetraaza-benzo[b]triphenylene-11-yl)phenylmethanone

1,10-phenanthroline-5,6-dione

4-benzoylbenzene-1,2-diamine

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