(E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

Base Information

Chemical Name:(E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester
CAS No.:150047-80-6
Molecular Formula:C₂₅H₂₂O₄
Molecular Weight:386.447
Hs Code.:

Synonyms:(E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

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Technology Process of (E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

There total 3 articles about (E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 2495-35-4,25036-21-9
benzylacrylate

: 150047-79-3
(E)-3-(7-Bromo-2-naphthalenyl)-2-propenoic acid ethyl ester

: 150047-80-6
(E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

Guidance literature:: With palladium diacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 85 ℃; for 16h;
DOI:10.1016/S0040-4020(01)90219-4

Reference yield:

: 58556-75-5
2,7-dibromonaphthalene

: 150047-80-6
(E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Pd(OAc)2, Pd(PPh₃)4, Et₃N / dimethylformamide / 7 h / 85 °C

2: 41 percent / Pd(OAc)2, Pd(PPh₃)4, Et₃N / dimethylformamide / 16 h / 85 °C

With palladium diacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)90219-4

Reference yield:

: 140-88-5,9003-32-1
ethyl acrylate

: 150047-80-6
(E,E)-3,3'-(2,7-Naphthalenylene)-bis-2-propenoic acid ethyl phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Pd(OAc)2, Pd(PPh₃)4, Et₃N / dimethylformamide / 7 h / 85 °C

2: 41 percent / Pd(OAc)2, Pd(PPh₃)4, Et₃N / dimethylformamide / 16 h / 85 °C

With palladium diacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)90219-4