(4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

Base Information

Chemical Name:(4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one
CAS No.:143955-40-2
Molecular Formula:C₂₀H₂₉NO₄S
Molecular Weight:379.521
Hs Code.:

Synonyms:(4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

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Chemical Property of (4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

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Technology Process of (4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

There total 4 articles about (4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 882-33-7
diphenyldisulfane

: 143955-40-2
(4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine, sulfuryl chloride / tetrahydrofuran / 1 h / Ambient temperature

2: tetrahydrofuran; CH₂Cl₂ / 1.5 h / Ambient temperature

3: 1.) i-Pr₂NEt, Bu₂BOTf, 2.) Et₂AlCl / 1.) CH₂Cl₂, 0 deg C, 45 min, 2.) -78 deg C, 1 h

With pyridine; sulfuryl dichloride; di-n-butylboryl trifluoromethanesulfonate; diethylaluminium chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/p19960001935

Reference yield:

: 931-59-9
benzenesulfenyl chloride

: 143955-40-2
(4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; CH₂Cl₂ / 1.5 h / Ambient temperature

2: 1.) i-Pr₂NEt, Bu₂BOTf, 2.) Et₂AlCl / 1.) CH₂Cl₂, 0 deg C, 45 min, 2.) -78 deg C, 1 h

With di-n-butylboryl trifluoromethanesulfonate; diethylaluminium chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/p19960001935

Reference yield:

: 77877-19-1,165657-81-8
N-isopropyl oxazolidinone

: 143879-15-6
(α-phenylthio)valeraldehyde

: 143955-40-2
(4S)-3-<(2R,3S,4S)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

: 143879-17-8
(4S)-3-<(2R,3S,4R)-3-Hydroxy-2-methyl-4-phenylsulfanyl-1-oxoheptyl>-4-(1-methylethyl)-1,3-oxazolidin-2-one

Guidance literature:: With di-n-butylboryl trifluoromethanesulfonate; diethylaluminium chloride; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 2) -78 deg C, 1 h;
DOI:10.1016/S0040-4039(00)74262-6