cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

Base Information

Chemical Name:cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine
CAS No.:89848-09-9
Molecular Formula:C₂₉H₃₀Cl₂N₆O₃
Molecular Weight:581.502
Hs Code.:

Synonyms:cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

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Chemical Property of cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

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Technology Process of cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

There total 6 articles about cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 89872-79-7
cis-1-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-4-(4-nitrophenyl)piperazine

: 89848-09-9
cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

Guidance literature:: With thiophene; hydrogen; palladium on activated charcoal; In methanol; 2-methoxy-ethanol; at 50 ℃; Heating;
DOI:10.1021/jm00373a015

Reference yield:

: 100-00-5
4-chlorobenzonitrile

: 89848-09-9
cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / K₂CO₃ / dimethylsulfoxide / 120 °C

2: 80 percent / H₂, thiophene / 5percent Pd/C / 2-methoxy-ethanol; methanol / 50 °C / Heating

With thiophene; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; 2-methoxy-ethanol; dimethyl sulfoxide;
DOI:10.1021/jm00373a015

Reference yield:

: 67914-86-7,854372-78-4
cis-[2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl]methyl methanesulfonate

: 89848-09-9
cis-1-<4-<4-<<2-(2,4-dichlorophenyl)-2-(1H-1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-4-yl>methoxy>phenyl>-1-piperazinyl>benzenamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) Me₂SO, 1 h, 2.) Me₂SO, 80 deg C, 5 h

2: 70 percent / NaOH / butan-1-ol / Heating

3: 50 percent / K₂CO₃ / dimethylsulfoxide / 120 °C

4: 80 percent / H₂, thiophene / 5percent Pd/C / 2-methoxy-ethanol; methanol / 50 °C / Heating

With thiophene; sodium hydroxide; hydrogen; sodium hydride; potassium carbonate; palladium on activated charcoal; In methanol; 2-methoxy-ethanol; dimethyl sulfoxide; butan-1-ol;
DOI:10.1021/jm00373a015