(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

Base Information

Chemical Name:(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide
CAS No.:863544-73-4
Molecular Formula:C₅₈H₇₇NO₅Si₂
Molecular Weight:924.424
Hs Code.:

(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

Synonyms:(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

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Chemical Property of (Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

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Technology Process of (Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

There total 7 articles about (Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885022-89-9
di-O-tert-butyldiphenylsilyl-(S)-tyrosinol

: 209119-07-3
(Z)-12-(Tetrahydro-pyran-2-yloxy)-dodec-9-enoic acid

: 863544-73-4
(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

Guidance literature:: (Z)-12-(Tetrahydro-pyran-2-yloxy)-dodec-9-enoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In acetonitrile; at -5 ℃; for 1h;

di-O-tert-butyldiphenylsilyl-(S)-tyrosinol; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1021/jm051226l

Reference yield:

: 1931-63-1
methyl ester of azelaic acid aldehyde

: 863544-73-4
(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: KHMDS / tetrahydrofuran / -78 °C

2.1: aq. LiOH / tetrahydrofuran

3.1: isobutyl chloroformate; N-methylmorpholine / acetonitrile / 1 h / -5 °C

3.2: 491 mg / acetonitrile / 1 h / 20 °C

With 4-methyl-morpholine; lithium hydroxide; potassium hexamethylsilazane; isobutyl chloroformate; In tetrahydrofuran; acetonitrile; 1.1: Wittig olefination;
DOI:10.1021/jm051226l

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 863544-73-4
(Z)-N-[(1S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-1-[[4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]phenyl]methyl]ethyl]-12-[(tetrahydro-2H-pyran-2-yl)oxy]-9-dodecenamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: (COCl)2; DMSO; Et₃N

2.1: KHMDS / tetrahydrofuran / -78 °C

3.1: aq. LiOH / tetrahydrofuran

4.1: isobutyl chloroformate; N-methylmorpholine / acetonitrile / 1 h / -5 °C

4.2: 491 mg / acetonitrile / 1 h / 20 °C

With 4-methyl-morpholine; lithium hydroxide; oxalyl dichloride; potassium hexamethylsilazane; dimethyl sulfoxide; triethylamine; isobutyl chloroformate; In tetrahydrofuran; acetonitrile; 1.1: Swern oxidation / 2.1: Wittig olefination;
DOI:10.1021/jm051226l