(1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

Base Information

Chemical Name:(1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine
CAS No.:322392-02-9
Molecular Formula:C₂₁H₂₉NO₃
Molecular Weight:343.466
Hs Code.:

Synonyms:(1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

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Chemical Property of (1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

Chemical Property:

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Technology Process of (1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

There total 4 articles about (1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [2-(3,4-Dimethoxy-phenyl)-but-(E)-ylidene]-((R)-2-methoxy-1-phenyl-ethyl)-amine

: 322392-02-9
(1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

: [(R)-2-(3,4-Dimethoxy-phenyl)-butyl]-((R)-2-methoxy-1-phenyl-ethyl)-amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h;
DOI:10.1016/S0957-4166(00)00343-8

Reference yield:

: 5703-21-9
3,4-dimethoxyphenylacetaldehyde

: 322392-02-9
(1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / Na₂SO₄ / diethyl ether / 0.08 h

2.1: LDA / tetrahydrofuran / 1 h / -78 °C

2.2: tetrahydrofuran / 2 h / -78 °C

3.1: NaBH₄ / methanol / 0.5 h / 20 °C

With sodium tetrahydroborate; sodium sulfate; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; 1.1: Substitution / 2.1: deprotonation / 2.2: Alkylation / 3.1: Reduction;
DOI:10.1016/S0957-4166(00)00343-8

Reference yield:

: 64715-85-1,91298-74-7,127180-88-5
(R)-2-methoxy-1-phenylethylamine

: 322392-02-9
(1R,2'S)-(-)-N-[2'-(3,4-dimethoxyphenyl)butyl]-2-methoxy-1-phenylethylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / Na₂SO₄ / diethyl ether / 0.08 h

2.1: LDA / tetrahydrofuran / 1 h / -78 °C

2.2: tetrahydrofuran / 2 h / -78 °C

3.1: NaBH₄ / methanol / 0.5 h / 20 °C

With sodium tetrahydroborate; sodium sulfate; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; 1.1: Substitution / 2.1: deprotonation / 2.2: Alkylation / 3.1: Reduction;
DOI:10.1016/S0957-4166(00)00343-8