2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

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Chemical Name:2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol
CAS No.:870460-36-9
Molecular Formula:C₄₀H₆₄O₆S₂
Molecular Weight:705.077
Hs Code.:

Synonyms:2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

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Chemical Property of 2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

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Technology Process of 2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

There total 4 articles about 2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 870460-35-8
2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethanol

: 23288-49-5
(4,4'-isopropylidenedithio)bis[2,6-di-tert-butylphenol]

: 870460-36-9
2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 65 ℃; for 18.5h;

Reference yield:

: 41820-27-3
Δ³-dimethyl dihydromuconate

: 870460-36-9
2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine; osmium(VIII) oxide / water; acetone; tert-butyl alcohol / 18.25 h / 0 - 20 °C

1.2: 0.5 h

2.1: toluene / 24 h / Heating / reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

3.2: 0 °C

4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 18.5 h / 0 - 65 °C

With 4-methyl-morpholine; osmium(VIII) oxide; lithium aluminium tetrahydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; acetone; toluene; tert-butyl alcohol; 4.1: Mitsunobu reaction;

Reference yield:

: 528560-51-2
3,4-dihydroxy-hexanedioic acid dimethyl ester

: 870460-36-9
2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-{2-[2-ethoxy-5-(2-hydroxy-ethyl)-[1,3]dioxolan-4-yl]-ethoxy}-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 24 h / Heating / reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

2.2: 0 °C

3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 18.5 h / 0 - 65 °C

With lithium aluminium tetrahydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; 3.1: Mitsunobu reaction;