2,2',4,4'-Tetrachlorodibenzyl ether

Base Information

• Chemical Name: 2,2',4,4'-Tetrachlorodibenzyl ether
• CAS No.: 207974-13-8
• Molecular Formula: C₁₄H₁₀Cl₄O
• Molecular Weight: 336.045
• European Community (EC) Number: 960-302-1
• Nikkaji Number: J1.955.086I
• Mol file: 207974-13-8.mol

Synonyms:2,2',4,4'-Tetrachlorodibenzyl ether;207974-13-8;2,4-dichloro-1-[(2,4-dichlorophenyl)methoxymethyl]benzene;2,2,4,4-TETRACHLORODIBENZYLETHER;2,4-DICHLORO-1-{[(2,4-DICHLOROPHENYL)METHOXY]METHYL}BENZENE;1,1'-(Oxydimethanediyl)bis(2,4-dichlorobenzene) (Bis-(2,4-dichlorobenzyl) Ether);Bis-(2,4-dichlorobenzyl) Ether;2,4-Dichlorobenzyl Alcohol Impurity G;SCHEMBL7888003;NWYHVMDKERUNLM-UHFFFAOYSA-N;FT-0609097;EN300-222525;4,4'-oxybis(methylene)bis(1,3-dichlorobenzene);2,4-dichloro-1-[(2,4-dichlorophenyl)(methoxy)methyl]benzene

Chemical Property of 2,2',4,4'-Tetrachlorodibenzyl ether

Chemical Property:

• PSA: 9.23000
• LogP: 6.01700
• XLogP3: 5.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 335.945626
• Heavy Atom Count: 19
• Complexity: 250

Purity/Quality:

98%Min ^*data from raw suppliers

2,4-dichloro-1-[(2,4-dichlorophenyl)methoxymethyl]benzene 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1Cl)Cl)COCC2=C(C=C(C=C2)Cl)Cl

Technology Process of 2,2',4,4'-Tetrachlorodibenzyl ether

There total 2 articles about 2,2',4,4'-Tetrachlorodibenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,4-dichlorobenzyl trimethysilyl ether (624286-51-7) → C14H10Cl4O (207974-13-8)

Guidance literature:

With sulfuric acid; silica gel; In hexane; at 20 ℃; for 0.75h;

DOI:10.1055/s-2003-41469

Reference yield:

(2,4-dichlorophenyl)methanol (1777-82-8) + 2,4-Dichlorobenzyl chloride (94-99-5) → C14H10Cl4O (207974-13-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/op000085o

Reference yield:

C14H10Cl4O (207974-13-8) → 2,4 dichlorobenzoic acid (50-84-0) + 2,4-dichlorobenzaldeyhde (874-42-0)

Guidance literature:

With nitric acid; sodium nitrite; In water; at 90 ℃;

DOI:10.1021/op000085o

upstream raw materials:

2,4-dichlorobenzyl trimethysilyl ether

(2,4-dichlorophenyl)methanol

2,4-Dichlorobenzyl chloride

Downstream raw materials:

2,4 dichlorobenzoic acid

2,4-dichlorobenzaldeyhde