C₄₉H₆₉N₇O₈S

Base Information

Chemical Name:C₄₉H₆₉N₇O₈S
CAS No.:205498-79-9
Molecular Formula:C₄₉H₆₉N₇O₈S
Molecular Weight:916.195
Hs Code.:

C<sub>49</sub>H<sub>69</sub>N<sub>7</sub>O<sub>8</sub>S

Synonyms:C₄₉H₆₉N₇O₈S

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Chemical Property of C₄₉H₆₉N₇O₈S

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Technology Process of C₄₉H₆₉N₇O₈S

There total 9 articles about C₄₉H₆₉N₇O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 133120-91-9
(2R,3R,4S)-dolaproine-(S)-dolaphenine

: 172837-42-2
(S)-1-((S)-2-{[(S)-2-((S)-2-Benzyloxycarbonylamino-3-methyl-butyrylamino)-3-methyl-butyryl]-methyl-amino}-3-methyl-butyryl)-pyrrolidine-2-carboxylic acid

: 205498-79-9
C₄₉H₆₉N₇O₈S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jm970800t

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 205498-79-9
C₄₉H₆₉N₇O₈S

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / diisopropylethylamine, tripyrrolidinobromophosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

2: H₂, 12N HCl / 10percent Pd/C / methanol / 16 h / 760 Torr / Ambient temperature

3: 84 percent / diisopropylethylamine, (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

4: 3N HCl / dioxane / 5 h

5: 82 percent / diisopropylethylamine, tripyrrolidinobromophosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

With hydrogenchloride; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jm970800t

Reference yield:

: 42417-65-2
Z-MeVal-OH

: 205498-79-9
C₄₉H₆₉N₇O₈S

Guidance literature:: Multi-step reaction with 7 steps

1: 76 percent / diisopropylethylamine, tripyrrolidinobromophosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

2: 99 percent / H₂, 12N HCl / 10percent Pd/C / methanol / 16 h / 760 Torr / Ambient temperature

3: 93 percent / diisopropylethylamine, tripyrrolidinobromophosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

4: H₂, 12N HCl / 10percent Pd/C / methanol / 16 h / 760 Torr / Ambient temperature

5: 84 percent / diisopropylethylamine, (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

6: 3N HCl / dioxane / 5 h

7: 82 percent / diisopropylethylamine, tripyrrolidinobromophosphonium hexafluorophosphate / CH₂Cl₂ / 1 h / Ambient temperature

With hydrogenchloride; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jm970800t