(S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

Base Information

Chemical Name:(S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester
CAS No.:166321-87-5
Molecular Formula:C₃₄H₅₃N₅O₁₂
Molecular Weight:723.821
Hs Code.:

Synonyms:(S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

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Chemical Property of (S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

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Technology Process of (S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

There total 4 articles about (S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 10466-72-5
N-(2,4-dinitrophenyl)-ε-amino-n-caproic acid

: 69984-05-0
(S)-2-((S)-2-Amino-4-tert-butoxycarbonyl-butyrylamino)-pentanedioic acid di-tert-butyl ester

: 166321-87-5
(S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/ac00115a023

Reference yield:

: 16874-06-9
di-tert-butyl L-glutamate

: 166321-87-5
(S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / CH₂Cl₂

2: 100 percent / H₂ / 10percent Pd on carbon

3: 74 percent / dicyclohexylcarbodiimide, Hydroxybenzotriazole, diisopropylethylamine / dimethylformamide

With hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ac00115a023

Reference yield:

: C₂₁H₂₆N₂O₈

: 166321-87-5
(S)-2-{(S)-4-tert-Butoxycarbonyl-2-[6-(2,4-dinitro-phenylamino)-hexanoylamino]-butyrylamino}-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / CH₂Cl₂

2: 100 percent / H₂ / 10percent Pd on carbon

3: 74 percent / dicyclohexylcarbodiimide, Hydroxybenzotriazole, diisopropylethylamine / dimethylformamide

With hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ac00115a023