methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

Base Information

Chemical Name:methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate
CAS No.:197516-50-0
Molecular Formula:C₂₀H₂₃NO₅
Molecular Weight:357.406
Hs Code.:

Synonyms:methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

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Chemical Property of methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

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Technology Process of methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

There total 1 articles about methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2417-73-4
methyl 2-bromomethylbenzoate

: 20839-80-9
(4-methoxybenzylamino)acetic acid methyl ester

: 197516-50-0
methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

Guidance literature:: With triethylamine; In diethyl ether; for 16h; Heating;
DOI:10.1021/jo034160f

Reference yield: 81.0%

: 197516-50-0
methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

: 4-hydroxy-2-(4-methoxy-benzyl)-1,2-dihydro-isoquinoline-3-carboxylic acid methyl ester

Guidance literature:: With sodium hydride; tert-butyl alcohol; In toluene; for 12h; Heating;
DOI:10.1021/jo034160f

Reference yield:

: 197516-50-0
methyl 2-{N-(methoxycarbonylmethyl)-N-[(4-methoxyphenyl)methyl]aminomethyl}benzoate

: 610273-36-4
3-hydroxy-4-methoxycarbonylmethyl-2-(4-trifluoromethylphenyl)-2H-pyrazolo[4,3-c]isoquinolinium inner salt

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / t-BuOH; NaH / toluene / 12 h / Heating

2: 48 percent / 4-toluenesulfonic acid hydrate / ethanol / 18 h / Heating

3: 96 percent / trifluoroacetic acid / 8 h / Heating

4: 46 percent / K₂CO₃ / dimethylformamide / 25 °C

With p-toluenesulfonic acid monohydrate; sodium hydride; potassium carbonate; trifluoroacetic acid; tert-butyl alcohol; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo034160f