methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Base Information

Chemical Name:methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate
CAS No.:1423700-11-1
Molecular Formula:C₂₁H₂₅BO₄
Molecular Weight:352.238
Hs Code.:

Synonyms:methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Suppliers and Price of methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate 97%
1g
$ 475.00

Total 2 raw suppliers

Chemical Property of methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Methyl2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

There total 11 articles about methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 5359-48-8
methyl 2-(4-bromophenyl)-2-phenylacetate

: 73183-34-3
bis(pinacol)diborane

: 1423700-11-1
methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; for 4h; Inert atmosphere; Reflux;

Reference yield: 66.0%

: 1609003-96-4
methyl 2-phenyl-2-(4-(((trifluoromethyl)sulfonyl)oxy)phenyl)acetate

: 73183-34-3
bis(pinacol)diborane

: 1423700-11-1
methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 120 ℃; for 3h; Inert atmosphere; Sealed tube;
DOI:10.1021/ja503163k

Reference yield:

: 22979-35-7
Methyl phenyldiazoacetate

: 1423700-11-1
methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: [tris(2,4-di-tert-butylphenyl)phosphine]gold chloride; silver hexafluoroantimonate / dichloromethane / 0.02 h / 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 0.25 h / 0 - 20 °C / Inert atmosphere

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 3 h / 120 °C / Inert atmosphere; Sealed tube

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; silver hexafluoroantimonate; [tris(2,4-di-tert-butylphenyl)phosphine]gold chloride; potassium acetate; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ja503163k