4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

Base Information

Chemical Name:4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol
CAS No.:1022953-72-5
Molecular Formula:C₁₉H₂₂N₂O₅S
Molecular Weight:390.46
Hs Code.:

Synonyms:4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

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Chemical Property of 4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

Chemical Property:

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Technology Process of 4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

There total 4 articles about 4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-83-1
(2-hydroxyethyl)(methyl)amine

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1001395-59-0
N-phenylsulfonyl-5-hydroxy-6-methoxy-1H-indole

: 1022953-72-5
4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

Guidance literature:: (2-hydroxyethyl)(methyl)amine; formaldehyd; In ethanol; at 65 ℃; for 0.0833333h;

N-phenylsulfonyl-5-hydroxy-6-methoxy-1H-indole; In ethanol; at 70 ℃; for 2h;

Reference yield:

: 5-(benzyloxy)-6-methoxy-1-(phenylsulfonyl)-1H-indole

: 1022953-72-5
4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; cyclohexene / palladium 10% on activated carbon / ethanol; water / 0.08 h / 150 °C / Microwave irradiation

2.1: ethanol / 0.08 h / 65 °C

2.2: 2 h / 70 °C

With hydrogenchloride; cyclohexene; palladium 10% on activated carbon; In ethanol; water;

Reference yield:

: 4790-04-9
5-benzyloxy-6-methoxy-indole

: 1022953-72-5
4-{[(2-hydroxyethyl)(methyl)amino]methyl}-6-methoxy-1-(phenylsulfonyl)-1H-indoI-5-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 20 °C

2.1: hydrogenchloride; cyclohexene / palladium 10% on activated carbon / ethanol; water / 0.08 h / 150 °C / Microwave irradiation

3.1: ethanol / 0.08 h / 65 °C

3.2: 2 h / 70 °C

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; cyclohexene; palladium 10% on activated carbon; In ethanol; dichloromethane; water;