(Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1217436-00-4
Molecular Formula:C₁₆H₂₃BO₃
Molecular Weight:274.168
Hs Code.:

Synonyms:(Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 4 articles about (Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 66021-98-5
(o-methoxyphenyl)-1-propyne

: 73183-34-3
bis(pinacol)diborane

: 1217436-00-4
(Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: bis(pinacol)diborane; With 1-dodecyl-3-methylimidazole-2-thione; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

(o-methoxyphenyl)-1-propyne; With methanol; In tetrahydrofuran; at 20 ℃; for 24h; regioselective reaction; Inert atmosphere; sealed tube;
DOI:10.1039/b919515g

Reference yield: 83.0%

: 7732-18-5
water

: 66021-98-5
(o-methoxyphenyl)-1-propyne

: 73183-34-3
bis(pinacol)diborane

: 1217436-00-4
(Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With rac-SIPHOS; copper(II) bis(trifluoromethanesulfonate); caesium carbonate; at 20 ℃; regioselective reaction;
DOI:10.1016/j.cclet.2017.04.031

Reference yield: 61.0%

: 3698-28-0
2-allylanisole

: 73183-34-3
bis(pinacol)diborane

: 1217436-00-4
(Z)-2-(1-(2-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With C₆H₁₄Cl₂Ni₂; lithium tert-butoxide; at 100 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1038/s41929-021-00658-2