tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate

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Chemical Name:tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate
CAS No.:1018473-30-7
Molecular Formula:C₂₁H₂₇N₇O₂
Molecular Weight:409.491
Hs Code.:

Synonyms:tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate

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Chemical Property of tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate

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Technology Process of tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate

There total 2 articles about tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 515813-02-2
tert-butyl (3-bromo-4-methylphenyl)carbamate

: 1018473-23-8
(6-(5-amino-3-methylpyrazol-1-yl)pyrimidin-4-yl)methylamine

: 1018473-30-7
tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate

Guidance literature:: With caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 120 ℃; for 48h; High-pressure tube;

Reference yield:

: 1018473-22-7
C₈H₈ClN₅

: 1018473-30-7
tert-butl 4-methyl-3-(3-methyl-1-(6-methylaminopyrimidin-4-yl)-1H-pyrazol-5-ylamino)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: water; isopropyl alcohol / 4 h / 50 °C / Sealed tube

2: caesium carbonate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 48 h / 120 °C / High-pressure tube

With caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; water; isopropyl alcohol;