(3-BroMo-4-Methyl-phenyl)-carbaMic acid tert-butyl ester

Base Information

Chemical Name:(3-BroMo-4-Methyl-phenyl)-carbaMic acid tert-butyl ester
CAS No.:515813-02-2
Molecular Formula:C12H16BrNO2
Molecular Weight:286.169
Hs Code.:
Mol file:515813-02-2.mol

Synonyms:tert-Butyl (3-bromo-4-methylphenyl)carbamate;Carbamic acid,(3-bromo-4-methylphenyl)-,1,1-dimethylethyl ester;QC-8575;

Suppliers and Price of (3-BroMo-4-Methyl-phenyl)-carbaMic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(3-Bromo-4-methyl-phenyl)carbamicAcidtert-ButylEster
100mg
$ 45.00

J&W Pharmlab
(3-Bromo-4-methyl-phenyl)-carbamicacidtert-butylester 97%
500mg
$ 549.00

J&W Pharmlab
(3-Bromo-4-methyl-phenyl)-carbamicacidtert-butylester 97%
5g
$ 3998.00

J&W Pharmlab
(3-Bromo-4-methyl-phenyl)-carbamicacidtert-butylester 97%
1g
$ 998.00

Crysdot
tert-Butyl(3-bromo-4-methylphenyl)carbamate 95+%
100g
$ 677.00

Chemcia Scientific
(3-Bromo-4-methyl-phenyl)-carbamicacidtert-butylester ＞98%
25 G
$ 240.00

Alichem
tert-Butyl(3-bromo-4-methylphenyl)carbamate
100g
$ 670.32

AK Scientific
tert-Butyl(3-bromo-4-methylphenyl)carbamate
25g
$ 384.00

Total 6 raw suppliers

Chemical Property of (3-BroMo-4-Methyl-phenyl)-carbaMic acid tert-butyl ester

Chemical Property:

Boiling Point:297.1±33.0 °C(Predicted)
PKA:13.20±0.70(Predicted)
PSA：41.82000
Density:1.356±0.06 g/cm3(Predicted)
LogP:4.11810

Purity/Quality:

99%, ^*data from raw suppliers

(3-Bromo-4-methyl-phenyl)carbamicAcidtert-ButylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3-BroMo-4-Methyl-phenyl)-carbaMic acid tert-butyl ester

There total 2 articles about (3-BroMo-4-Methyl-phenyl)-carbaMic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7745-91-7
3-bromo-4-methylaniline

: 34619-03-9
tert-butyldicarbonate

: 515813-02-2
tert-butyl (3-bromo-4-methylphenyl)carbamate

Guidance literature:: With sodium hydroxide; In water; at 20 ℃; for 5h; Heating / reflux;

Reference yield: 63.0%

: 7745-91-7
3-bromo-4-methylaniline

: 24424-99-5
di-tert-butyl dicarbonate

: 515813-02-2
tert-butyl (3-bromo-4-methylphenyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2008.06.048

Reference yield: 100.0%

: 515813-02-2
tert-butyl (3-bromo-4-methylphenyl)carbamate

: 74-88-4
methyl iodide

: 877064-95-4
tert-butyl (3-bromo-4-methylphenyl)(methyl)carbamate

Guidance literature:: tert-butyl (3-bromo-4-methylphenyl)carbamate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 20h;