methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

Base Information

Chemical Name:methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside
CAS No.:165804-60-4
Molecular Formula:C₂₂H₃₁F₃N₂O₅
Molecular Weight:460.494
Hs Code.:

methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-<trifluoroacetyl-<(1R)-phenylethyl>amino>-α-D-erythro-hexopyranoside

Synonyms:methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

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Chemical Property of methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

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Technology Process of methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

There total 6 articles about methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 91704-27-7
N-((2S,5R,6S)-5-Amino-6-methoxy-tetrahydro-pyran-2-ylmethyl)-2,2,2-trifluoro-N-((R)-1-phenyl-ethyl)-acetamide

: 165804-60-4
methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

Guidance literature:: With sodium hydrogencarbonate; In methanol; at 10 ℃; for 3h; ultrasonic bath;

Reference yield:

: 91704-05-1
(2S)-2-[N-trifluoroacetyl-N-((R)-phenylethyl)aminomethyl]-3,4-dihydro-2H-pyran

: 165804-60-4
methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NOCl, 2.) 1,3,5-trimethylpyrazole / 1.) CH₂Cl₂, -78 deg C

2: 1.35 g / NaBH₃CN / acetic acid / 1.5 h / 15 °C

3: 1.10 g / H₂ / 10percent Pd-C / acetic acid / 3 h / 750.06 Torr / Ambient temperature

4: 65 percent / NaHCO₃ / methanol / 3 h / 10 °C / ultrasonic bath

With 1,3,5-trimethyl-1H-pyrazole; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; nitrosylchloride; palladium on activated charcoal; In methanol; acetic acid;

Reference yield:

: 2-<(1R)-phenylethylaminomethyl>-3,4-dihydro-2H-pyran

: 165804-60-4
methyl 2-(tert-butyloxycarbonylamino)-2,3,4,6-tetradeoxy-6-amino>-α-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 1 h / 0 °C

2: 1.) NOCl, 2.) 1,3,5-trimethylpyrazole / 1.) CH₂Cl₂, -78 deg C

3: 1.35 g / NaBH₃CN / acetic acid / 1.5 h / 15 °C

4: 1.10 g / H₂ / 10percent Pd-C / acetic acid / 3 h / 750.06 Torr / Ambient temperature

5: 65 percent / NaHCO₃ / methanol / 3 h / 10 °C / ultrasonic bath

With 1,3,5-trimethyl-1H-pyrazole; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; nitrosylchloride; palladium on activated charcoal; In pyridine; methanol; acetic acid;