cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

Base Information

Chemical Name:cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate
CAS No.:389084-25-7
Molecular Formula:C₁₆H₃₀O₅Si
Molecular Weight:330.497
Hs Code.:

Synonyms:cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

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Chemical Property of cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

Chemical Property:

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Technology Process of cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

There total 3 articles about cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 171866-13-0
cis,cis-3-hydroxy-5-methyl-carbonyloxy-cyclohexyl acetate

: 389084-25-7
cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

Guidance literature:: With triethylamine; dmap; In dichloromethane; at 25 ℃; for 36h;
DOI:10.1021/ja0685708

Reference yield:

: 50409-12-6,13314-30-2
cis,cis-1,3,5-trihydroxycyclohexane

: 389084-25-7
cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / 0 - 20 °C

2: 90 percent / 0.1 M sodium phosphate buffer; Porcine Liver Esterase / 12 h / 30 °C / pH 7

3: 90 percent / DMAP; Et₃N / CH₂Cl₂ / 12 h / 20 °C

With porcine liver esterase; dmap; sodium phosphate buffer; triethylamine; In pyridine; dichloromethane;
DOI:10.1021/jo016141g

Reference yield:

: 327622-76-4
cis,cis-3,5-di(methylcarbonyloxy)cyclohexyl acetate

: 389084-25-7
cis,cis-3-(methyl-carbonyloxy)-5-(tert-butyl-dimethylsilyloxy)-cyclohexyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 0.1 M sodium phosphate buffer; Porcine Liver Esterase / 12 h / 30 °C / pH 7

2: 90 percent / DMAP; Et₃N / CH₂Cl₂ / 12 h / 20 °C

With porcine liver esterase; dmap; sodium phosphate buffer; triethylamine; In dichloromethane;
DOI:10.1021/jo016141g