1-phenylethyl 4-methoxyperoxybenzoate

Base Information

Chemical Name:1-phenylethyl 4-methoxyperoxybenzoate
CAS No.:77787-73-6
Molecular Formula:C₁₆H₁₆O₄
Molecular Weight:272.301
Hs Code.:

Synonyms:1-phenylethyl 4-methoxyperoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenylethyl 4-methoxyperoxybenzoate

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Technology Process of 1-phenylethyl 4-methoxyperoxybenzoate

There total 3 articles about 1-phenylethyl 4-methoxyperoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-41-4,27536-89-6
ethylbenzene

: 77787-73-6
1-phenylethyl 4-methoxyperoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: AIBN, O₂ / 24 h / 110 °C

2: 10percent NaOH, NaCl / CCl₄; H₂O / 0.17 h / 40 °C

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); oxygen; sodium chloride; In tetrachloromethane; water;
DOI:10.1021/ja00401a026

Reference yield:

: 3071-32-7
1-phenylethyl hydroperoxide

: 100-07-2
4-methoxy-benzoyl chloride

: 77787-73-6
1-phenylethyl 4-methoxyperoxybenzoate

Guidance literature:: With sodium hydroxide; sodium chloride; In tetrachloromethane; water; at 40 ℃; for 0.166667h; Yield given;
DOI:10.1021/ja00401a026

Reference yield:

: 98-85-1,13323-81-4
1-Phenylethanol

: 77787-73-6
1-phenylethyl 4-methoxyperoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / conc. H₂SO₄, 90percent H₂O₂ / 1.) 0 deg C, 2 h, 2.) 22-28 deg C, 4 h

2: 10percent NaOH, NaCl / CCl₄; H₂O / 0.17 h / 40 °C

With sodium hydroxide; sulfuric acid; dihydrogen peroxide; sodium chloride; In tetrachloromethane; water;
DOI:10.1021/ja00401a026