1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

Base Information

Chemical Name:1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime
CAS No.:884320-31-4
Molecular Formula:C₂₇H₂₆BrNO₄
Molecular Weight:508.412
Hs Code.:

Synonyms:1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

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Chemical Property of 1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

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Technology Process of 1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

There total 12 articles about 1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 884320-39-2
1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one

: 884320-31-4
1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 15h; Heating;
DOI:10.1021/ja0602997

Reference yield:

: 884320-42-7
2-(2-bromo-5-methoxyphenyl)prop-2-en-1-ol

: 884320-31-4
1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / Ph₃P; imidazole; I₂ / CH₂Cl₂ / 0.5 h / 0 °C

2.1: potassium hexamethylisilazide; DMPU / tetrahydrofuran; toluene / 1 h / 20 °C

2.2: 54 percent / tetrahydrofuran; toluene; various solvent(s) / 1 h / 20 °C

3.1: 75 percent / NH₂OH*HCl; NaOAc / ethanol / 15 h / Heating

With 1H-imidazole; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hydroxylamine hydrochloride; iodine; sodium acetate; potassium hexamethylsilazane; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/ja0602997

Reference yield:

: 884320-33-6
1-bromo-2-(3-iodoprop-1-en-2-yl)-4-methoxybenzene

: 884320-31-4
1-[2-(2-bromo-5-methoxy-phenyl)-allyl]-7-methoxy-1-(3-methoxy-phenyl)-indan-2-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylisilazide; DMPU / tetrahydrofuran; toluene / 1 h / 20 °C

1.2: 54 percent / tetrahydrofuran; toluene; various solvent(s) / 1 h / 20 °C

2.1: 75 percent / NH₂OH*HCl; NaOAc / ethanol / 15 h / Heating

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; hydroxylamine hydrochloride; sodium acetate; potassium hexamethylsilazane; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/ja0602997