13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Base Information

Chemical Name:13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane
CAS No.:147688-15-1
Molecular Formula:C₂₀H₃₂N₂O₆
Molecular Weight:396.484
Hs Code.:

Synonyms:13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

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Chemical Property of 13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Chemical Property:

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Technology Process of 13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

There total 4 articles about 13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 25711-25-5
benzyl aziridine-1-carboxylate

: 66943-05-3
1,4,7,10-tetraoxa-15-azacyclopentadecane

: 147688-15-1
13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Guidance literature:: In toluene; acetonitrile; for 24h; Heating;

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 147688-15-1
13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; tetrabutylammomium bromide / water; toluene / 10 h / 70 °C / Inert atmosphere

2: acetic acid; palladium on activated charcoal; hydrogen / methanol / 12 h / 20 °C / 7500.75 Torr / Autoclave; Inert atmosphere

3: acetonitrile; toluene / 24 h / Reflux; Inert atmosphere

With palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; acetic acid; sodium hydroxide; In methanol; water; toluene; acetonitrile;
DOI:10.1039/c9dt01512d

Reference yield:

: 93407-96-6
2-(((benzyloxy)carbonyl)amino)ethyl 4-methylbenzenesulfonate

: 147688-15-1
13-Benzyloxycarbonylaminoethylen-1,4,7,10-tetraoxa-13-azacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / NaH / tetrahydrofuran / 20 h / 40 °C

2: 78 percent / acetonitrile; toluene / 24 h / Heating

With sodium hydride; In tetrahydrofuran; toluene; acetonitrile;