N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide

Base Information

Chemical Name:N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide
CAS No.:150223-34-0
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:
DSSTox Substance ID:DTXSID401203782

Synonyms:DTXSID401203782;N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide;150223-34-0

Suppliers and Price of N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:345.15762283
Heavy Atom Count:25
Complexity:405

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CCNC(=O)C2=C(C(=CC=C2)OC)OC)OC

Technology Process of N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide

There total 1 articles about N-[2-(3,4-Dimethoxyphenyl)ethyl]-2,3-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1521-38-6
2,3-dimethoxybenzoic acid

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 150223-34-0
2,3-dimethoxy-benzoic acid-(3,4-dimethoxy-phenethylamide)

Guidance literature:: 2,3-dimethoxybenzoic acid; 2-(3,4-dimethoxyphenyl)-ethylamine; With dmap; In tetrahydrofuran; at 25 ℃; for 0.0833333h; Inert atmosphere;

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 45 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01868

Reference yield: 85.0%

: 150223-34-0
2,3-dimethoxy-benzoic acid-(3,4-dimethoxy-phenethylamide)

: C₁₉H₂₂INO₅

Guidance literature:: 2,3-dimethoxy-benzoic acid-(3,4-dimethoxy-phenethylamide); With silver trifluoromethanesulfonate; In dichloromethane; at 25 ℃; for 0.0333333h; Inert atmosphere;

With iodine; In dichloromethane; at 25 ℃; for 12h; regioselective reaction; Darkness; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01868