(S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

Base Information

Chemical Name:(S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate
CAS No.:1620161-69-4
Molecular Formula:C₁₇H₂₄N₂O₄S
Molecular Weight:352.455
Hs Code.:

Synonyms:(S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

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Chemical Property of (S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

Chemical Property:

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Technology Process of (S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

There total 1 articles about (S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 27317-69-7
N-tert-butoxycarbonyl-L-alanyl-L-alanine

: 108-98-5
thiophenol

: 1620161-69-4
(S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield: 84.0%

: 4306-24-5
Gly-Leu-Tyr

: 1620161-69-4
(S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

: 1620161-81-0
(6S,9S,15S,18S)-18-(4-hydroxybenzyl)-15-isobutyl-2,2,6,9-tetramethyl-4,7,10,13,16-pentaoxo-3-oxa-5,8,11,14,17-pentaazanonadecan-19-oic acid

Guidance literature:: With benzotriazol-1-ol; In dimethyl sulfoxide; at 20 ℃; for 25h; Reagent/catalyst; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield:

: 1620161-69-4
(S)-S-phenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanethioate

: 1620162-23-3
cyclo[-Ala-Ala-Gly-Leu-Tyr-]

: 1620162-64-2
C₄₆H₆₆N₁₀O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-ol / dimethyl sulfoxide / 25 h / 20 °C / Inert atmosphere

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 0 - 20 °C

4: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 18 h / 20 °C / Inert atmosphere

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol501669n