5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

Base Information

Chemical Name:5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester
CAS No.:182758-13-0
Molecular Formula:C₁₅H₁₄Br₂I₃NO₅
Molecular Weight:828.801
Hs Code.:

Synonyms:5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

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Chemical Property of 5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

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Technology Process of 5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

There total 1 articles about 5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 89180-84-7
2,5-Dibromopentanoic Acid Bromide

: 154921-11-6
dimethyl 5-amino-2,4,6-triiodo-1,3-benzenedicarboxylate

: 182758-13-0
5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

Guidance literature:: In N,N-dimethyl acetamide; for 20h; Ambient temperature;
DOI:10.1016/0040-4020(96)00668-0

Reference yield: 73.0%

: 182758-13-0
5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

: 182758-05-0
5-(3-Bromo-2-oxo-piperidin-1-yl)-2,4,6-triiodo-isophthalic acid dimethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl acetamide; for 0.5h; Ambient temperature;
DOI:10.1016/0040-4020(96)00668-0

Reference yield:

: 182758-13-0
5-(2,5-Dibromo-pentanoylamino)-2,4,6-triiodo-isophthalic acid dimethyl ester

: 5-(3-Hydroxy-2-oxo-piperidin-1-yl)-2,4,6-triiodo-isophthalic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / K₂CO₃ / N,N-dimethyl-acetamide / 0.5 h / Ambient temperature

2: 71 percent / acetic acid / 21 h / Heating

3: 76 percent / NaOCH₃, methanol / 17 h / Ambient temperature

With methanol; sodium methylate; potassium carbonate; In N,N-dimethyl acetamide; acetic acid;
DOI:10.1016/0040-4020(96)00668-0