4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

Base Information

Chemical Name:4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine
CAS No.:1032235-45-2
Molecular Formula:C₂₅H₁₉N₃O₂
Molecular Weight:393.445
Hs Code.:

Synonyms:4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

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Chemical Property of 4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

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Technology Process of 4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

There total 1 articles about 4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 447399-94-2
4′-(4-hydroxymethylphenyl)-2,2′:6′,2′′-terpyridine

: 814-68-6,25189-84-8
acryloyl chloride

: 1032235-45-2
4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

Guidance literature:: With triethylamine; In butanone; at 0 ℃;
DOI:10.1039/b716011a

Reference yield: 71.0%

: ammonium hexafluorophosphate

: 1032235-45-2
4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

: [Ru(4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine)Cl₃]

: [Ru(4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine)2](PF₆)2

Guidance literature:: With N-ethylmorpholine;; In methanol; under inert atm. ligand was added to Ru complex in MeOH along with N-ethylmorpholine, soln. was filtered, soln. NH4PF6 in MeOH was added; ppt. was filtered and recrystd. from acetone-MeCN soln. and dried in vacuo; elem. anal.;
DOI:10.1039/b716011a

Reference yield: 70.0%

: 1032235-45-2
4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine

: 14898-67-0
ruthenium(III) chloride trihydrate

: [Ru(4'-(4-acryloyloxymethylphenyl)-2,2':6',2''-terpyridine)Cl₃]

Guidance literature:: In ethanol; under inert atm. RuCl3*3H2O and ligand in EtOH were refluxed for 8 h; react. mixt. was cooled, ppt. was filtered, washed with MeOH, water and Et2O and dried in vacuo;
DOI:10.1039/b716011a